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Instrumentation

  

Metrohm 831

Metrohm 831 Coulometer Karl-Fischer Titrator: determines very small amounts of water and gives an unmistakable presentation of the course of titration in form of a curve showing μg water against time.

 

Mini Block

MiniBlock XT: flexible easy-to-use reaction block designed for parallel synthesis and reaction screening.


VAC purification

VAC Solvent Purification and Drying Unit: Obtains dry solvents without the hazards of distillation stills.

 

Buchi Kugelrohr

Buchi Kugelrohr Distillation/Oven: Distill relatively small volumes of liquids with high boiling points under greatly reduced pressure.

 

Microwave reactor

CEM Microwave Reactor: High frequency electric fields provide an alternate form of rapid heating. Accelerated reaction rates, milder reaction conditions and higher chemical yields are its popular features.

 

Combi-flash

Teledyne Isco Combi-Flash: Fast and efficient separation of small molecules. Automated collection of fractions which are free of contamination.

 

HPLC

Waters HPLC: Normal/Reverse phase separation of organic molecules using a binary pump and UV detector. Can also be used for analysis of chiral compounds.

 

Shared Equipment available for use by the CSF:

Brucker Bio-TOF III High Resolution Mass Spectrometer

Brucker Esquire 3000 + MS-MS Spectrometer

Agilent GC-Mass Spectrometer

Varian Inova 500 MHz NMR Spectrometer with triple axis gradients (actively shielded)

Varian Inova 400 MHz NMR Spectrometer with Z axis gradients

Varian Mercury 300 MHz NMR with Z-axis gradients

H-Cube Flow Hydrogenator